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GCMS analysis results, sample AD23901, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23901 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067467–000067480

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23901.D Vial: 6 Acq On : 17 Oct 2001 6:11 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 4 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.62 ug/1 162784 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, -hydroxy-4-methyl- 116 C6H12O2 000123-42-2 53 2 Acetic acid. Zi,i-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Propane, iethyl-2-(1-methylethoxy 116 C7H16O 017348-59-3 28 4 Acetic a; d, cyano-, 1,1-dimethylet 141 C7H11NO2! 001116-98-9 17 Abundance Scan 296 (7.755 min): 23901 .D (-) Tm7z 427^5 100.00% 4(3

59 5000

101 ------------------ 7.^ " 7.60 " 7.» " aOO " ’ ' ' 83 ........................ P ' ‘ ' I ' ‘ ' I ' I I I ' • > • I ‘ m/z 59.05 55.34% n/z-> 10 20 30 40 60 70 80 90 100 110 Abundance #64275:2-Pentanone. 4-hydroxy-4-tnethyl- 4(3

5000 59 7.40 7.60 7.80 8.00 ..................... '....................... 15 31 101 I I, 83 I ' ' I ' ‘‘I ' I ‘ ‘ ' I ' ' ' ' I ' I ' ' ' ' 1 ' ' ' ' I ' Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3^: Acetic acid, 1,1 -dimethylethyl ester 4(3

7.40 7.60 7.80 8.00 5000 57 18.20% 101 15 I ' I ‘ ‘ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ■ ‘ ■ I ' Tife-> 10 TO 30 40 ' "so" 60 70 80 90 100 110 Abundance #3378: Propane, 2-methyl-2-(1-methylethoxy)- 59 7.40 7.60 7.80 8.00 m/z 41.05 8.76% 5000 41 101 27 I I I ' ' ' ' I ' ' ‘ ' I ‘ I I ' ■nfe-> 10 20 30 40 50 60 to’ " m" "90''' 166 '' i-io 7.40 7.60 7.80 8.00

23901.D NP101901.M Tue Oct 23 12:47:31 2001 Page 4

NYC-WTC_000067478

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NYC-WTC_000067478Source: NYC Law Department, mirrored locally

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