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GCMS analysis results, sample AD23901, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23901 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067467–000067480

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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Scanned page image, NYC-WTC_000067479
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NYC 9/11 Public Portal Document

Librairy Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23901.D Vial: 6 Acq On : 17 Oct 2001 6:11 pm Operator: 209 GALOS Sample : gc/ms unknown Inst s GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP Calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.51 ug/1 50893 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForra CAS# Qual 1 1,4-Dichlorobeja:zene-d4 150 C6C12D4 003855-82-1 56 2 Benzenamine, /2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 22 3 Benzene-1,2y3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 17 4 Benzenamip»e, 2-methyl-5-nitro-- 152 C7H8N2O2 000099-55-8 14 Abundance / Scan 718 (11.629 min): 23901 .D (-) m/z 149.90 100.00% 1!i0

500) 115 52 78 11.20 11.40 11.60 11.80 12.00 38 . I. , ,11 87 I 111' ■ • 111 ■ ' I'' ‘' I -1-14*1-1 m/z 151.90 66.97% nZz-> 30 40 50 60 70 80 90 100 110 120 130 150 160 ^bundance #9593:1,4-DichIorobenzene-d4 1$0

5000 78 115 -r* R 11.20 11.40 11.60 11.80 12.00 52 m/z 114.90 37.88% 35 87 I'''' I nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 IK) Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 1Q6 1Ji2

1120' '1'1 !4o' '1'1 .To 11 iso 'izob 5000 “mTz 77795 17777% 51 94 66 tiA:-> 30 40 50 60 70 80 90 160 116 1^ IM 140 lOT 160 Abundance #9592: Benzen8-1.2,3.4-d4-. 5,6-dichloro- 1!i0 11.20 11.40 11,60 11.80 12.00 “m/z 52.00 14.40% 115 5000 52 78

uZz-> 30 35 1 40 ■ I 50 z ■'' I ■''' I' • 60 70 87 I I • " ' I' 80 90 A 100 110 120 130 140 150 160 11'20 1i!40 U.K)' 11'so ‘1'2'00'

23901.D NP101901.M Tue Oct 23 12:47:33 2001 Page 5

NYC-WTC_000067479

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NYC-WTC_000067479Source: NYC Law Department, mirrored locally

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