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GC/MS analysis results for sample AD23360, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23360 conducted on October 16, 2001.

NYC-WTC_000088585–000088603

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088596
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23360.D Vial: 18 Acq On : 10 Oct 2001 5:55 am Operator: 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise - Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.50 ug/1 46178 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 fentative ID MW MolForm CAS# Qual

1 1,4-Dichwrobenzene-d4 150 C6C12D4 003855-82-1 47 2 Benzene/1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 22 3 Benzof/lran, 7-chloro- 152 C8H5C1O 024410-55-7 9 4 Biph^ylene 152 C12H8 000259-79-0 9 ^bundance Scan 717 (11.626 min): 23360.D (-) m/z 150.00 100.00% 1!>0

5000 115

52 78 11.20 11.40 11.60 11.80 12.00 ........... ,1 m/z 151.90 66.04% Tl/Z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1'i0

115 _ 1818181 ' ' I ' ' 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 43.85% 35 ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 \bundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- liiO I I I I . I I I . , I /1 |V,,, I, , ,

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 "m/z 77795 16.83%

87

Ti/z-> 30 35 I ' I ' ' ' ' I ' ' ' ‘ I ' ' ‘ ‘ I ' 40 50 60 70 1 ' I ' ' ' ' I ' ' ' ' I ' 80 90 100 A 110 120 130 140 150 160 <\bundance #10136: Benzofuran, 7-chloro- I ' ' ' ' I ' ' ' ' H ' ' ' I ' ' 152 11.20 11.40 11.60 11.80 12.00 m/z 52/^ 15.94%

5000 89

63 35 49 .2 125 I I ' ' ‘ ' I ' ‘ ‘ ' P ' ' ■nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20'11.40 11.60 11.80 12.00

23360.D NP091101.M Thu Oct 11 13:13:07 2001 Page 5

NYC-WTC_000088596

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NYC-WTC_000088596Source: NYC Law Department, mirrored locally

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