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GC/MS analysis results for sample AD23342, Oct 19 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23342 conducted on October 19, 2001.

NYC-WTC_000088671–000088682

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088681
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23342.D Vial: 11 Acq On : 19 Oct 2001 1:58 am Operator: 209 GTkLOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration■Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.51 ug/1 44682 1,4-Dichlorobenzehe-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 78 2 Benzene-1,2y3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 40 3 Benzenamijre, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 14 4 Benzald^lyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 <\bundance Z Scan 717 (11.626 min): 23342.D (-) m/z 149.90 100.00% 1!i0

5000 115 78 52 11.20 11.40 11.60 11.80 12.00 . 40 I . I.. . '' I''' H '''' 11' I' I' m/z 151.90 70.38% TiZz~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 150

5000 52 78 115 T R 11.20 11.40 11.60 11.80 12.00 m/z 115.00 39754% 35 ... 1,1,,.... TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150

115 11.20 11.40 11.60 11.80 12.00 CT 52 78 “m/z 78.05 26.24%

35 87 I T-p-r-n-p- I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 106 152 11.20 11.40 11.60 11.80 12.00 "m/z 52.00 15.55%

5000

Tl/Z-> 51

' I ' ' ' ' I ' ' ' ' I ' 30 40 50 60 66

70 ...... 80 90 94

100 110 120 130 140 150 160 1 11.20 11.40 11.60 11.80 12.00

23342.D NP091101.M Fri Oct 19 10:13:31 2001 Page 3

NYC-WTC_000088681

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NYC-WTC_000088681Source: NYC Law Department, mirrored locally

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