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GC/MS analysis results for sample AD23342, Oct 19 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23342 conducted on October 19, 2001.

NYC-WTC_000088671–000088682

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088680
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23342.D Vial: 11 Acq On : 19 Oct 2001 1:58 am Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise - Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************:»;************************ Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.09 ug/1 96286 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanonp< 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 45 2 2-Propanplf, 2-methyl- 74 C4H10O 000075-65-0 17'. 3 5-Hexen42-one 98 C6H10O 000109-49-9 9 4 3-Hy^/oxy-2-pentanone____________ 102 C5H10O2 003142-66-3 9 fiSundancT^*^ Scan 295 (7.752 min): 23342.D (-) m7z 4^705 100.00% 4(3

5000

10 20 30 40 50 59

I 70 83 ' ' ' I ’ ''' ' I ' ' ' ' I ' ' ' ' I '' ‘ 60 80 ' I ' 90 101

100 110 m7z 740 4 7.60 59.05 7.80 8.00 53.69% I"

Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl-

5000- 59 7.40 7.60 7.80 8.00 m/z 101.05 18.71% 27 101 83 . ..... h'-J-T-i—I—I—r-r-1—7—y-i-H—I—I—|— 10 20 30 40 50 60 70 80 90 100 110 '\bundance #62575: 2-Propanol, 2-methyl- 50 __________ ,_______ ' ' I ' ' ' ' I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I ' _MO__7tO__A8O__aOO_^_ 553 m/z 58.05 17717% 31 41

jL. 15 I, , , , j, , , , ,2^, ,1, 4 nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one r i I I I I 1 I I I t I [ I I I I I I I I I'l I 413 7.40 7.60 7.80 8.00 m/z 41.05 8.12% 5000-

55 38 I 50 I 83 98 ' I I ' ' ‘ ' I ' I ' ‘ ' I ' ' ' ' I ' I ‘ ' I ' ' ' ' I ' ‘ ‘ I ' ' ' ' I ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

23342.D NP091101.M Fri Oct 19 10:13:29 2001 Page 2

NYC-WTC_000088680

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NYC-WTC_000088680Source: NYC Law Department, mirrored locally

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