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GC/MS analysis results for sample AD23360, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23360 conducted on October 16, 2001.

NYC-WTC_000088585–000088603

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088597
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23360.D Vial: 18 Acq On : 10 Oct 2001 5:55 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ***************************************************************** * * ****** Peak Number 6 1,3-Hexanediol, 2-ethyl- Concentration. Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.51 1.04 ug/1 96658 Chrysene-dl2 33.12

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 1,3-Hexa .ediol, 2-ethyl- 146 C8H18O2 000094-96-2 25 2 Oxiran^ 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 25 3 1-He; :ne, 5-methyl- 98 C7H14 003524-73-0 1'6 4 2-Un, iecene, 10-methyl- 168 C12H24 000000-00-0 16 Abundance Scan 2665 (29.509 min): 23360.D (-) m/z 56700 16^700% 5b

5000 4 73 I I I I I I I I , / I\ ,Q I I I

129 257 J .41 .b. I 143l5717l185i992n j 312 29.20 29.40 29.60 29.80 T 'I "-'I I m/z5679548.03% TiZz-> 4bundance 20 40 60 53 80 100 120 140 160 180 200 220 240 260 280 300 #66450:1.3-Hexanediol, 2-ethyl- ft S3 27 I 73 29,20 29,40 29,60 29.80 m/z 43.05 40.05% 3 1,,^. 1.14129 r ''' I'''' I'''' I nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ^bundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 5 41 29,20 29.40 29.60 29.80 5000 m/z 41.05 33.10% 73

Ti/z-> 20 40 60 J. 113128 I'''' I'''' I'''' I'''' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 I'''' I' ’ *' I

Abundance #63239:1-Hexene, 5-methyl- 53 29,20 29,40 29,60 29,80 41 m/z 73.00 30.62%

5000

JJi 27

n/z-> 20 40 60 98 I'''' I'''' I I'''' I I' ’ *' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 1 29.20 29.40 29.60 29.80

23360.D NP091101.M Thu Oct 11 13:13:09 2001 Page 6 •

"NYC-Wfc_000088597 '

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NYC-WTC_000088597Source: NYC Law Department, mirrored locally

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