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GC/MS analysis results for sample AD23360, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23360 conducted on October 16, 2001.

NYC-WTC_000088585–000088603

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088598
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23360 .D Vial: 18 Acq On : 10 Oct 2001 5:55 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.65 0.88 ug/1 81655 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl t^tradecanoate (myristate) 284 C18H36O2; 000000-00-0 72 2 1-Pentane, 2,4-dimethyl- 98 C7H14 002213-32-3 35 3 Octac^canoic acid, butyl ester 340 C22H44O2 000123-95-5 32 4 2-Methyl-N-1-tridecene 196 C14H28 018094-01-4 32 Abundance Scan 2898 (31.648 min); 23360.D (-) m/z 56700 100.00% 5|B

4- 73 129 285

jUu 185 241 267 | 31.40 31.60 31.80 32.00 340 P”'' ' I m/z 57700 48.69% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53

5000 229 31.40 31.60 31.80 32.00 73 211 m/z 43700 447150% 129 284 -r-rp-rTTyJ-rTTT-TTTTjTTT^^ •prrrrp-r TTp-TTT-p'T-Tnq-TTYrjT-rr^^ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #63263: 1-Pentene, 2,4-dimethyl- —iir^iii^iiiii I I Dp 1

31.40 31.60 31.80 32.00 4' m7z 41.05 38.89% 5000

, 83 98 ' I' I * “ ' I'''' I I ' '' ' I'' '' I' ' '' I -n/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester ^1^11 /Pl 11J11\ I i'YV 11 V 5^ 31.40 31.60 31.80 32.00 m/z 55700 32.64% 5000- 285 340 73 267 129

I'''' I'' 185 I I " I' " ' I' " ' I'' " I " " I' " ' I'' ‘' I A ' ' I ' ' Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23360.D NP091101.M Thu Oct 11 13:13:12 2001 Page 7

NYC-WTC_000088598

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NYC-WTC_000088598Source: NYC Law Department, mirrored locally

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