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GC/MS analysis results for sample AD23272, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.

NYC-WTC_000088456–000088484

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088471
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23272.D vial: 22 Acq On : 12 Oct 2001 10:39 pm Operator: 209 GALOS Sample : gc/ms unknown., Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Butyl tetradecanoate (myristat Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.64 7.05 ug/1 754481 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl te adecanoate (myristate) 284 C18H36O2 000000-00-0 64 2 Octadecjfanoic acid, 2-methylpropyl e 340 C22H44O2: 000646-13-9 60 3 Octa^canoic acid, butyl ester 340 C22H44O2: 000123-95-5 32 4 2-^hyl-Nt 1-tridecene_____________ 196 C14H28 018094-01-4 27 \bundapde Scan 2898 (31.642 min): 23272.0 (-) m/z 56700 100.00% 55

5000 4' 73 I

129 A

■n/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #40186: Butyl tetradecanoate (myristate) .xX. 340 m/z 31.40 31.60 31.80 32.00 SYTOO 50759%

53

5000 229 31.40 31.60 31.80 32.00 211 m/z 43705 40769% , 129 284

■n/z-> 40 UmXr 60 80 p-rT-rp-T-rTT 100 120 140 160 180 200 220 240 260 280 300 320 340 ‘ J''' I ‘' I'''' I

^bundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

31.40 31.60 31.80 32.00 5000 m/z 41.05 34.96% 285

xU 267 J 185 241 340 l' ' '' I ' ' ' ' I ‘ ' I ' ' ' ' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48208: Octadecanoic acid, butyl ester 5|S 31.40 31.60 31.80 32.00 m/z 73.00 30.85% Sign 285 73 340

a 129 267 97 185 241 I I I y+rTTp-n-rf I I '' ' ' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23272.D NP091101.M Mon Oct 15 09:42:07 2001 Page 9

NYC-WTC_00008847l‘ '

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NYC-WTC_000088471Source: NYC Law Department, mirrored locally

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