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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089431
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23836.D Vial: 16 Acq On : 31 Oct 2001 5:09 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1-Hexene, 2-methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 29.45 4.09 ug/1 639549 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 22methyl- 98 C7H14 006094-02-6 27 2 Butyl hexa^canoate 312 C20H40O2i 000000-00-0 25 3 Oxirane, X3-bis(1-methylethyl)-, t 128 C8H166 054644-32-5 23 4 Cyclbpeyanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 17 \bundance ' Scan 2659 (29.451 min): 23836.D (-) Tm/z 56.00 100.00% 5b

5000 4 73 7 129 257 I 312 29.20 29.40 29.60 29.80 ■ 111 j 11 11 'p I /tf. m/z 57.00 50.84% Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ^bundance #63261; 1 -Hexene, 2-methyl- 53

41 5000 29,20 29,40 2^60 29.80 27 m/z 43.00 39.81% ,7.....98.................................. ........... . .............. Ti/z-> 20 40 60 80 1t^ 120 140 1^' 180 200 ^0 2^ 260 286 '360 ' Abundance #44549: Butyl hexadecanoate 55

29.20 29.40 29.60 29.80 553 258 • m/z 41.05 35.06% 73 240 312 129 I I 15717iJ^5 214 -rpTi I I I I *1 r I . I . I I . I I i' I . I 'i I j 1 I I . I I I I I I 1 Ir I " '' I tt/2-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- JUbv.... —■^29.20^ 29.40 29.60 29.80 ~ ■^41= “m/z—54-795------ 3-0T65 %

5000 J I 73 , j 113128 . ■ ' .■

Tdz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 28o' 'sOO ' 29.20 29.40 29.60 29.80

23836.D NP103001.M Thu Nov 01 13:27:09 2001 Page 7

NYC-Wf C_000089431

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NYC-WTC_000089431Source: NYC Law Department, mirrored locally

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