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GC/MS analysis results for sample AD23323, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23323 conducted on October 15, 2001.

NYC-WTC_000088290–000088315

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088302
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23323.D Vial: 16 Acq On : 12 Oct 2001 4:47 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1-Hexene, 5-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

29.51 3.67 ug/1 378663 Chrysene-dl2 33.12

Hit# of 5 jntative ID MW- MolForm CAS# Qual

1 1-Hexene,/5-methyl- 98 C7H14 003524-73-0 27 2 Cyclobut^e, 1, lTdimethyl-2-octyl- 196 C14H28 062338-30-1 27 3 Butyl ixadecanoate 312 C20H40O2i 000000-00-0 25 4 Cyclo; intanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 23 Abundance / Scan 2665 (29.508 min): 23323. D (-) m/z- 56.00 107700% 5b

5000 4' 73 129 257 P ' '•^1 ' ' I 29.20 29.40 29.60 29.80 m/z 57700 48733% Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63239:1-Hexene, 5-methyl- 53 41

5000 ' ' I ' ' 29.20 29.40 29.60 29.80 27 70 m/z 43.05 38.05% 7 •r, nr? -pX^yVrr?TTn-rrTTn-rrp-rr.-p-rrrp-rrT^^

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance

5000 55 #21985: Cyclobutane, 1,1-dimethyl-2-octyl-

uU 29.20 29.40 29.60 29.80 m/z 41.05 74747% I

27 70 I I I 9/111125140 168 196 riVri^-nl^l-ii/i | r i i i | i i i i | i I i I '' ' * I p-r-r-q-m-q- n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 5 29.20 29.40 29.60 29.80 m/z 73.00 28.45% 258

240 312 7 ’29 Tl/Z-> I ' ' ' ' I ' ■TT-t-f-rr?Tp--rrV]‘T-r*1Y’-*rTp-rn-*p-rVT-p--rrT-]^^ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 A I''' r 29.20 29.40 29.60 29.80

23323.D NP091101.M Mon Oct 15 10:29:26 2001 Page 6

NYC-WTC_000088302

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NYC-WTC_000088302Source: NYC Law Department, mirrored locally

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