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GC/MS analysis results for sample AD23261, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23261 conducted on October 12, 2001.

NYC-WTC_000088098–000088114

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088106
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23261.D Vial: 7 Acq On 9 Oct 2001 7:13 pm Operator: 209 GALOS Sample g c/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 2 1,3-Hexanediol, 2-ethyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

29.51 0.62 ug/1 114450 Chrysene-dl2 33.13

Hit# of 5 'entative ID MW MolForm CAS# Qnal

1 1,3-Hex.^ediol, 2-ethyl- 146 C8H18O2 000094-96-2 37 2 1-Hex. e, 2-methyl- 98 C7H14 006094-02-6 27 3 Pental ecane, 8-methylene- 224 C16H32 055668-09-2 25 4 Oxi/ane, 2,3-bis(1-methylethyl)- , t 128 C8H16O 054644-32-5 23 Abundance Scan 2665 (29.510 min): 23261.D (-) m/z 56700 100.00%

5000 4 73 I mt '*29 257 239 29.20 29.40 29.60 29.80

Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 XX 312 T-X m/z 57.00 48.76% Abundance #8882:1,3-Hexanediol, 2-ethyl- 55

5000 73 M 29,20 29.40 29.60 29.80 m/z 43.05 38.84% 31 103 A I I' ''' r Xi „l r '' ' r ' '' I I '''' I' ''' I ''' ' I''' ' I' ''' I'' '' I •n/z-> 20 40 80 100 120 140 160 180 200 220 240 260 280 300 60 Abundance #1354:1-Hexene, 2-methyl- 5S

41 29.20 29.40 29.60 29.80 5000 m/z 41.05 37.39% A 27

•n/2-> 20 XVx 40 60 70

80 98 "h r '' ' r ' '' I ‘ ' I 100 120 140 160 180 200 220 240 260 280 300 I'''' I

Abundance #28775: Pentadecane, 8-methylene- 29.20 29.40 29.60 29.80 m/z 73.00 32.21% 5000

70 84

Tl/Z~> 27 I I' ''' I' 20 jULiXX 40 I '''' I'''' I'' 1' I''' ' I'' 60 196 224 I < < . . I rv.I I .I ■ ■ I I < 80 100 120 140 160 180 200 220 240 260 280 300 r '' ’ 1'''' I'' *' I'''' ( 1 29.20 29.40 29.60 29.80

23261.D NP091101.M Thu Oct 11 10:45:48 2001 Page 2

NYC-WTC_000088106

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NYC-WTC_000088106Source: NYC Law Department, mirrored locally

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