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GC/MS analysis results for sample AD23084, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23084 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087904–000087919

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT04 0l\23084.D Vial: 4 Acq On 4 Oct 2001 6:27 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,3-Hexanediol, 2-ethyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

29.53 0.50 ug/1 81020 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Hexanei ol, 2-ethyl- 146 C8H18O2 000094-96-2 37 2 Cyclopen .necarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 35 3 Cyclop tanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 35 4 Butyl .exadecanoate 312 C20H40O2 35 Abundance / Scan 2668 (29.532 min): 23084.0 (-)" i 1 55 A 5»w 41

129 239 257 __ a,.,,.... m/z-> 20 40 60 I 143157171 185 213 80.J00 120 140 160 _180 200 220 _240 260 280 300 XX 312 -Htt 29.20 29.40 29.60 29.80 m/z 57.00 45.72% Abundance #8882:1,3-HexanedioT, 2-ethyl-

T 5000 73 29.20 29.40 29.60 29.80 m/ z 41.05 42.42% 31 103 I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5218; Cyclopentanecarboxylic acid, 2-amino-, cis- 56

! 29.20 29.40 29.60 29.80 5000 m/z 43.05 37.41% I 30 69 82 100 129 .1 I ' ' ' ' I I ' ' ' ' 1 ' ' ' ‘ I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxytic acid. 2-amino-, trans- i 5l6 29.20 29.40 29.60 29.80 m/ z 73.00 34.14% 5000

30 69 82 100 129 ,1 1 ......J......... !m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23084.D NP091101.M Tue Oct 09 12:29:20 2001 Page 3

NYC-WTC_000087913

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NYC-WTC_000087913Source: NYC Law Department, mirrored locally

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