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GC/MS analysis results for sample AD22581, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22581 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087226–000087249

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22581.D vial; 9 Acq On ; 28 Sep 2001 8:16 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl hexadecanoate Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 29.54 1.24 ug/1 196085 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hexad^e^oate 312 C20H40O2 000000-00-0 59 2 Cycloperjb^ecarboxylic acid, 2-amin 12 9 C6H11NO2 037910-65-9 38 3 Cyclgp^tanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 38 4 Oxi^ne, 2,3-bis (1-methylethyl) - t 128 C8H16Q 054644-32-5 37 Abundance Scan 2668 (29,537 min); 22581 ,D (-) Tm/z 56.00 100.00% 5|B

5000 4' 73 I /I ’ I n- j .H., ...g^U^ lvT.143157171185199213 j :^.2O 29.40 29,60 29.80 312 ' I'''' I '''' I m/z 57.00 45.65% TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549; Butyl hexadecanoate 55

5000 258 I ' ' ' 29,20 29.40 29.60 29,80 73 240 312 m/z 129 43.05 35.76% L II I 157171^^ ¥jH-TM^yrTH-ryTTTTY’'TVT-ph-rTy^^ 214

uU I'' * • I TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5218; Cyclopentanecarboxylic acid, 2-amino-, cis- 53 J 29,20 29,40 29,60 29,80 5000 m/z 41.05 34.35%

30 ,1 tiA:-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #5212; Cyclopentanecarboxylic acid, 2-amino-, trans- _ / LAa I ' ' ' ' I ' ' ‘ ' I 5(6 29,20 29,40 29,60 29,80 m/z 73700 28.65% 5000

30 70 sz 100 129 ,1 Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 2120 29.40 29.60 29.80

22581.D NP091101.M Mon Oct 01 12:03:20 2001 Page 6

NYC-WTC_000087238

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NYC-WTC_000087238Source: NYC Law Department, mirrored locally

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