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GC/MS analysis results for sample AD23843, Nov 2 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23843 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089397–000089417

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089408
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT3001\23843.D Vial; 15 Acq On : 31 Oct 2001 4:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L Peak Number 4 Butyl hexadecanoate Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 29.45 1.50 ug/1 370974 Chrysene-dl2 33.06 Hit# of 5 'entative ID MW MolForm CAS# Qual ■ 1 Butyl he^decanoate 312 C2 0H40O2: 000000-00-0 52 . 2 0xiraney2,3-bis (1-methylethyl) - , t 128 C8H16O 054644-32-5 32 3 1-Hexenfe, 2-methyl- 98 C7H14 006094-02-6 27 ... 4 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2I _____ 040482^05-1 25. Abundance / Scan 2659 (29.454 min): 23843.D (-) pWz SYTOO 100700% 5h

5000 4' 73 257 I ' ' 312 29.20 29.40 29.60 29.80 '-I-'-... I. I Wz SYTOO 45.76% Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 (Kbundance #44549: Butyl hexadecanoate 5

253 258 RR u 29.20 29.40 29.60 29:80 73 240 312 129 m/z 43.05 38.96% 157171214 tVz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 53 41 f l I 1 I I 'Ti -i T| 29.20 29.40 29.60 29.80 5000 m/z 41.05 36.43% I nfe-> 20 40 T -.ll--------- 113128 - I'' 11'''I''' ■ I'■' ■ I' 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354:1-Hexene, 2-methyl- 53 : " 29,20\ 29.40 .- 29.60 29.801 "mTz 73700 29.00% 41 5000

27 70 I ,1 98 I ' ’ ' ' I ' ’ ' ' I ' ' ' ‘ I I'' '' 1''' ' 1''' ' 1' ‘* I' ‘' I ... ,,M......... Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23843.D NP103001.M Thu Nov 01 14:44:24 2001 . Page 4

NYC-WTC_OOo6894O8

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NYC-WTC_000089408Source: NYC Law Department, mirrored locally

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