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GC/MS analysis report for sample AD25792, Dec 2001

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DEP laboratory report documenting GC/MS results for sample AD25792 analyzed on December 6, 2001.

NYC-WTC_000070097–000070112

Folder label: “GCMS Scan X 10/30/01 An 11/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1901\25792.D Vial: 12 Acq On : 20 Nov 2001 2:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.45 0.98 ug/1 256018 Chrysene-dl2 33.05 Hit# of 5 Tenteative ID MW MolForm CAS# Qual 1 Butyl hexadexfanoate 312 C20H40O2! 000000-00-0 35 2 Oxirane, 2/3-bis(1-methylethyl) -, t 128 C8H16O 054644-32-5 32 3 1-Hexeney2-methyl- 98 C7H14 006094-02-6 27 4 1-Hexen^ 2,5-dimethyl- 112 C8H16 006975-92-4 27 Abundance Scan 2659 (29.452 tnin): 25792.D (-) m/z 56.00 100.00% 55

5000 41 73 257 .. ^29

TiZz-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #44549: Butyl hexadecanoate XL m/z 29.20 29.40 29.60 29.80 57.00 ft 48.12%

T 5000 258 29.20 29.40 29.60 29.80 240 312 41.05 40.54% L 7 ^29 m/z TTp-TTTp-iTl f ri 11 I /1 • I I I r J * I I k I I 11 •* I 1 I I 1 j , n I i I . J I .

nZz-> 20 40 60 80 100 120 140 160 180 200 220 240 2K) 280 300 Abundance #5067: Oxirane, 2,3-bis(1 -methylethyl)-, trans- 55 41 •f 29.20 29.40 29.60 29.80 5000- m/z 43.05 36.95% 73

■nfe-> 20 40 'BO J. 113128 ■p-rrrp-TT-i I' * ’' I p-n-rp-TTTj 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- 55 29.20 29.40 29.60 29.80 m/z 55.0.0 31.51% 41 50)0 27

IvA.,A, Tlfe-> 20 29.20 29.40 29.60 29.80

25792.D NP103001.M Wed Dec 05 15:19:49 2001 Page 2

NYC-WTC_000070106

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NYC-WTC_000070106Source: NYC Law Department, mirrored locally

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