GC/MS analysis report for sample AD25792, Dec 2001

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Library Search Contpound Report Data File ; C:\HPCHEM\1\DATA\NOV1901\25792.D vial: 12 Acq On : 20 Nov 2001 2:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. ----------------- -------- 7.70 0.57 ug/1 109361 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ’entative ID MW MolPorm CAS# Qual 1 2-Pentanphe, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetonyl 58 C3H6O 000067-64-1 12 3 2-PrgjgJanone, 1-cyclopropyl- 98 C6H10O 004160-75-2 9 4 Formal de, N,N-diethyl- 101 C5H11N0 000617-84-5 9 (\bundance f Scan 290 (7.704 min): 25792.D (-) Wz 42795 100.00%

5000

Tife-> nArTTTH- t 59

I,,,, I, < 111,1 ■. I 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 101 7.40 m/z 7.^' 59.05 L aoo' 49.35% Abundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 413

5000 7.^ 7,60 7,80 8.00 m/z 101.05 20.26% 31 83 101 73 pnfi|liii|iinr P*T TiZz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #62322: Acetone 43

7.40 7.60 7.80 8.00 5000 m/z 58.05 19.76% 58

Trr|llil|iinpirl|ll I" " I "I I‘ ' I'" ' I " " I" " I''" I ‘‘' 1“‘' I nfe-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #1306:2-Propanone, 1-cycIopropy^ 4)3 7.40 7.60 7.80 8.00 ra/z 41.05 9.33% 5000

55 29 . ...... . 4-p^ pTTTpT+rpTTTyrTTTJTrlTpTTTpTr^^ Tife-> 15 20 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 7.^‘ Zto' '7.^' 8.60

25792.D NP103001.M Wed Dec 05 15:19:42 2001 Page 1

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