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GCMS analysis results for sample AD24290, Nov 5 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24290 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068158–000068170

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068167
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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24289.D Vial: 10 Acq On : 1 Nov 2001 12:54 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.19 ug/1 166311 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 :ntative ID MW MolForm CAS# Qual

1 2-Pentan0ne, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 38 2 3-Hydrp^^-2-pentanone 102 C5H10O2 003142-66-3 9 3 Morp^line, 4-methyl- 101 C5H11NO 000109-02-4 9 4 Ace^c acid, cyano-, 1,1-dimethylet 141 C7H11NO2i 001116-98-9 9 ^bundanc8 Scan 289 (7.695 min): 24289.D (-) Tm/z 42.95 100.00% 4(3

59 5000 101 ' 7.^ 7.60 7.80 8.00

Tlfe-> .............. I . , , ■ I , . .?,l, 10 20 30 40 50 ..Mr 60 70 80 90 100 110 m/z 59.05 50.38% Abundance #64274:2-Pentanone. 4-hydroxy-4-methyl- 4|3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95i 24.63% 27

Tife-> 10 20 I I 30 «-r+ 40 5060 70 80 .... S-..... T.... 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59

7.40 7OT ZOT 8.66 5000 m/z 58.05 18.52% 45 15 1 I ‘ ‘ ‘ I ‘ ‘ 1 ' I, I I ‘ 66 73 84_______ 102 ■ 1 > • ■ • 1 • • • ■ I ■ * I ■ I I > 1 • I > nte-> ' 'l'o' ’ ' ' 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- , , I , , I , , , , 4(3 7.^ 7.60 7,80 8.00 m/z 41.00 7.64%

5000 101

, T Y,.,., 10 20 30 40 I 56 I ■ ■ 1 • • I • I • • 50 60 71 • ■ I'l ■ ■ • I • ■ ■ • I ■ • I I I 1 • ■ • I I

70 80 90 100 110 7407507^08^

24289.D NP103001.M Fri Nov 02 12:01:38 2001 Page 2

NYC-WTC_000068167

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NYC-WTC_000068167Source: NYC Law Department, mirrored locally

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