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GCMS analysis results for sample AD24290, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24290 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068158–000068170

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : Cs\HPCHEM\1\DATA\OCT3101\24289 .D Vial: 10 Acq On : 1 Nov 2001 12:54 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.51 ug/1 72098 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Ten tive ID MW MolForm CAS# Qual 1 1,4-Dichlo enzene-d4 150 C6C12D4 003855-82-1 94 2 Benzene- ,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 2H-1-Be: ^opyran-3-ol, 3,4-dihydro- 150 C9H10O2 021834-60-6 9 4 Benza 'ehyde, 2-hydroxy-5-methoxy- 152 C8H8O3 000672-13-9 9 Abundance Scan 712 (11.578 min); 24289.D (-) m/z 149.85 100.00% 1$O

5000 115 52 78 T r 38 45 11.20 11.40 11.60 11.80 12.00 m/z 151.85 77771% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 1ii0

5000 115 ... 78 1120 11.40 11.60 11.80 12.00 52 m/z 115.00 41.12% T Tl/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1.2,3,4-d4-, 5.6-dichloro- 1!>0

115 1120 11.40 11.60 11.80 12.00 5000 52 78 m/z 52.00 25.16%

35 87 I '' I''' ‘ I' ‘' I'' ‘' I ‘' I'''' 1 ‘ I ‘' I' .. Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 \........... ance #9708; 2H-1-Benzopyran-3-ol. 3,4-dihydro- T-rfVr 107 1$0 11.20 11.40 11.60 11,80 12.00 m/z 78.05 23.30% 553 78 119 131 I 89 I IT TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24289.D NP103001.M Fri Nov 02 12:01:40 2001 Page 3

NYC-WTC_000068168

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NYC-WTC_000068168Source: NYC Law Department, mirrored locally

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