GC/MS analysis report for sample AD25791, Nov 2001

NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25791.D Vial: 21 Acq On : 17 Nov 2001 10:32 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Libraiy : C;\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.06 ug/1 367793 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm / CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Morpho^ne, 4-methyl- 101 C5H11NO 000109-02-4 9 3 Acet^e 58 C3H6O 000067-64-1 9 4 Ace^c acid, cyano-, 1,1-dimethylet 141 C7H11NO2i 001116-98-9 9 Abundance Scan 288 (7.687 min): 25791 .D (-) Tm/z 43.00 100.00% 4)3

59 5000

101 ‘ 7.^ ‘zto' 8.00 I. 69 83 , I m/z 59.05 50.87% Tlfe-> 10 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 '7.^' '7.60 ZTO sS'" m/z 100.95 21.53%

.L- 27 101 .......................... I I 83 I '-r+ ..... mZz-> 10 20 30 40 a) 60 70 80 90 100 110 Abundance #1640: Morpholine. 4-methyl- 4)3

7.40 7.60 7.80 8.00 5000 ra/z 58.05 17.66% 101 71

mfe-> UCX™- i ■ I ■ > ■ ■ I • ■ 1 • I •' ■ ■ 11 10 20 30 40________________ 50 60 70 ' I ' • ' ' I ' ‘ 80 90 ‘ I ‘ 100 ‘ I 110 Abundance #62322: Acetone ■ '‘1'■''1■■■■.I 4)3 7.40 7.60 7.80 8.00 m7z 41.05 8.49% 5000 58 27 t-r-rr- I ‘ ' I ‘ ' I ' ' ‘ ' 1 ' ‘ ' I ' ' ' ' I mZz-> 10 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25791.D GCMS1126.M Thu Nov 29 12:20:46 2001 Page 1

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