GCMS analysis comments for sample AD28695, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC04 01\28695.D vial: 10 Acq On 4 Dec 2001 9:10 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.44 1.19 ug/1 223391 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hexa decanoate 312 C20H40O21 000000-00-0 53 2 1-Hexene,/5-methyl- 98 C7H14 003524-73-0 27 3 1-Hexene 2-methyl- 98 C7H14 006094-02-6 27 4 Oxirane/ 2,3-bis(1-methylethyl)- f t 128 C8H160 054644-32-5 23 Abundance * Scan 2657 (29.439 min): 28695.D (-) m/z 56.00 100.00% 55

5000 41 73 . 257

XL mi 129 1 ' i ' ' 11" 29.20 29.40 29.60 29.80 —।—। 1277116,143157171185199213 312 TIWWIIIHT m/z 57.00 51.96% mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 55

5000 258 ' ■ i ■ ■ • • i ■ ■ 29.20 29.40 29.60 29.80 73 240 312 m/z 41.05 42.80% 129 -p-rr-rp-r 1.. TUPmmg —. 1.. 157171195 214 TT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63238:1-Hexene, 5-methyl- 55 T ■ T■ ' TITTTrfrr 41 29.20 29.40 29.60 29.80 5000 m/z 43.05 41.74% 70

m/z-> Abundance 20 p-. rrp. . T । 40 55 60 p. । । । । । | 80 100 120 140 160 180 200 220 240 260 280 300 #1354:1-Hexene, 2-methyl- । । 1 I ri | I I I I |

A m/z 29.20 29.40 29.60 29.80 55.00 33.39% 41 5000

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m/z—> 1 —2.9....... ;.. I ■''' I' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 T A 29.20 29.40 29.60 29.80

28695.D GCMS1126.M Thu Dec 06 15:20:40 2001 Page 1

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