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← Document results/DEP Box 60/GCMS Scan X 10/2/01 An 10/17/01
Document / 11 pages

GCMS calibration table, Oct 17 2001

Machine-extracted title · confidence 90%

Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.

NYC-WTC_000067428–000067438

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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Scanned page image, NYC-WTC_000067435
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\LB.D vial: 2 Acq On : 17 Oct 2001 2:09 pm Operator: 209 GALOS San^le : lab blk 10/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.43 ug/1 45618 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol / 102 C6H14O 000626-93-7 83 2 2-Pentanol/^4-methyl- 102 C6H14O 000108-11-2 74 3 2-HexanqX (R) - 102 C6H14O 026549-24-6 43 4 2-He; 1, (S)- 102 C6H14O 052019-78-0 43 Wxindance Scan 184 (6.727 min): LB.D (-) m/z 44795 100.00% 4)5

5000

41 69 ' ' I rv'fT 6.40 6.60 6.80 7.00

nZz-> pultt ..... I,?S...... ......... m/z 10 15 20 25 30 35 40 45 50 55 K) 65 70 75 80 85 90 95 69.00 16.75% ^bundance #1792:2-Hexanol 4}

A/ 5000 6.40 6.60 6.80 7.00 “mTz 41.05 15.41% 5558 8487

jhi__ " I' ‘" I" I' I ‘' I ‘' I" " I ‘‘ I"'' I'''' I'' ‘' I ‘ Tife-> 10 15 20 25 30 35 40 45 50 55«)65 70 75 80 85 90 95 ^bundance #63545:2-Pentanol, 4-methyl- 4b ■ ‘ I ' ' ‘ ' I ' ‘ ‘ ' I ' ' ‘ ' I ' ' ‘ ' I 6.40 6.60 6.80 7.00 5000 m/z” 43.90 9.45%

69 27 3942 , 57 r"t|'ni Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794:2-Hexanol, (R)- a 4b 6.40 6.60 6.80 7.00 Wz 43.00 8.84% 5000

69 55_________I_________ 8487 ......... -TTTT-TTTTTTTTyrTTTpTT-lYrrrTp-rTT^^ m/z~> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

LB.D NP101901.M Tue Oct 23 12:52:51 2001 Page 2 NYC-WTC_000067435

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NYC-WTC_000067435Source: NYC Law Department, mirrored locally

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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