Laboratory report detailing GCMS analysis of sample AD22558 conducted on October 1, 2001.
NYC-WTC_000067428–000067438Folder label: “GCMS Scan X 10/2/01 An 10/17/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\LB.D vial: 2 Acq On : 17 Oct 2001 2:09 pm Operator: 209 GALOS San^le : lab blk 10/2 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.43 ug/1 45618 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol / 102 C6H14O 000626-93-7 83 2 2-Pentanol/^4-methyl- 102 C6H14O 000108-11-2 74 3 2-HexanqX (R) - 102 C6H14O 026549-24-6 43 4 2-He; 1, (S)- 102 C6H14O 052019-78-0 43 Wxindance Scan 184 (6.727 min): LB.D (-) m/z 44795 100.00% 4)5
5000
41 69 ' ' I rv'fT 6.40 6.60 6.80 7.00
nZz-> pultt ..... I,?S...... ......... m/z 10 15 20 25 30 35 40 45 50 55 K) 65 70 75 80 85 90 95 69.00 16.75% ^bundance #1792:2-Hexanol 4}
A/ 5000 6.40 6.60 6.80 7.00 “mTz 41.05 15.41% 5558 8487
jhi__ " I' ‘" I" I' I ‘' I ‘' I" " I ‘‘ I"'' I'''' I'' ‘' I ‘ Tife-> 10 15 20 25 30 35 40 45 50 55«)65 70 75 80 85 90 95 ^bundance #63545:2-Pentanol, 4-methyl- 4b ■ ‘ I ' ' ‘ ' I ' ‘ ‘ ' I ' ' ‘ ' I ' ' ‘ ' I 6.40 6.60 6.80 7.00 5000 m/z” 43.90 9.45%
69 27 3942 , 57 r"t|'ni Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794:2-Hexanol, (R)- a 4b 6.40 6.60 6.80 7.00 Wz 43.00 8.84% 5000
69 55_________I_________ 8487 ......... -TTTT-TTTTTTTTyrTTTpTT-lYrrrTp-rTT^^ m/z~> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00
LB.D NP101901.M Tue Oct 23 12:52:51 2001 Page 2 NYC-WTC_000067435
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NYC-WTC_000067739
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 25, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067979
Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067623
DEP lab report for GCMS analysis of sample AD23914 conducted on October 25, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069732
Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068400
Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000067940
Calibration data sheet listing surrogate compounds and retention times for GC/MS instrument used in TCLP testing on October 31, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069271
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000088491
Calibration data table for TCLP analysis using GC/MS standards processed on October 18, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000089030
GC/MS analysis report with TCLP calibration table data from October 16, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000067405
Record of a GCMS scan conducted at the World Trade Center site between October and November 2001.
Filed in the same folder
NYC-WTC_000067406
Gas chromatography-mass spectrometry analysis of sample AD22558 started October 1, 2001, identifying other unknown compounds.
Filed in the same folder
NYC-WTC_000067425
Log sheet recording liquid-liquid extraction parameters and sample processing details for October and November 2001.
Filed in the same folder
NYC-WTC_000067439
DEP lab report for GCMS analysis of sample AD23844 conducted on October 23, 2001, noting unknown compounds.
Filed in the same folder
NYC-WTC_000067453
DEP lab report for GCMS analysis of sample AD23900 conducted on October 23, 2001, noting unknown compounds.
Filed in the same folder