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GCMS calibration table for TCLP analysis, Nov 2 2001

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Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.

NYC-WTC_000067979–000067989

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\LB.D Vial: 2 Acq On : 31 Oct 2001 5:05 pm Operator: 209 GALOS Sample : 10/10 Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.44 ug/1 70079 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol 102 C6H14O 000626-93-7 83 2 2-Pentsmol, 4-methy1- 102 C6H14O 000108-11-2 74 3 Butaiie, 2-ethoxy- 102 C6H14O 002679-87-0 50 4 2-H9!fcanol, (R) - 102 C6H14O 026549-24-6 43 Abundance Z iScan 177 (6.666 min): LB.D (-) Wz 45.00 100.00% 463

5000

-ri-Tr< ' ■ pTrri-i-i m

Tife-> 56 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 T l”’*l m/z 6.40 6.60 6.80 7.00 i69.00 15.39% Abundance #63584:2-Hexanol 46

5000 6.40 6.60 6.80 7.00 69 m/z .41-05 11.55% “ I ®7 TiZz-> ^bundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 #63547:2-Pentanol, 4-methyl- 4|5 jM ' ' 6.^' 6.OT 6.^ 7.ro 5000 “m/z 44.00 10.96%

27 1““i ,..,.,,1..,... »,.lll 17 T rrTTJTTTTjllTTJTTTTpTTlyrrT^^ ®7 Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #63540: Butane, 2-ethoxy- 4t5 6.40 6.60 6.80 7.00 m/z ,42.95 10.23% 73 5000

27 87 102 I'"' I *'" 1' “ ‘ 1 * ‘ * J "' r "' I" >nZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 6.^ " ROT " Iso ' 7.00

LB.D NP103001.M Fri Nov 02 17:17:22 2001 Page 2

NYC-WTC_000067986

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NYC-WTC_000067986Source: NYC Law Department, mirrored locally

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GCMS sample extraction log table, Nov 2001 · Box DEP Box 60

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Multi-page laboratory log table recording sample extraction details including volumes and drip rates for GCMS analysis in November 2001.

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