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GC/MS analysis results for sample AD22656, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22656 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087349–000087362

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087359
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22656.D Vial: 15 Acq On : 29 Sep 2001 2:10 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L

Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.63 0.43 ug/1 55222 1,4-Dichlorobenzene-d4 11.78

Hit# Of 5 ntative ID MW MolForm CAS# Qual

1 3-HexanQK 102 C6H14O 000623-37-0 83 2 3-Pent^ol, 2-methyl- 102 C6H14O 000565-67-3 38 3 4-He{<tanol 116 C7H16O 000589-55-9 22 4 BqXanamide, 3-methyl- 101 C5H11NO 000541-46-8 9 Wsund^e Scan 173 (6.632 min): 22656.D (-) m/z 59.05 100.00% 5^ 55

73 5000 43 ^1 I 86 6S__64o2Z6EZ6^^ZZSZL i..4|lili|...n 4+ t 4n7z 55.00 77.38% Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance ■ #63530:3-Hexanol 5(9

55 73 5000 6.20 6.40 6.60 6.80 7.00 31 m/z 73.00 51.17% 27 " I' " ' I'''' I " " I' I " I 45 84 44 ' I " " I " '' I " " I " " I' Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #1781:3-Pentanol, 2-methyl- 5|9

6.20 6.40 6.60 6.80 7.00 5000 31 73 m/ Z 43.00 24.50% 27

tt/z-> 5 10 15 .4. . ....... ............ 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 69

Abundance #64376: 4-Heptanol $ 6.20 440 ieo iso 7.^ 73 “m/z 41.05 18.85%

553 43 27 31 15 ,i59 69 I P"' n I r T ■HT»7TTTrpTTrn+ 11' " • I' I 'I I ."I111 tt/2-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80 7.00

22656.D NP091101.M Fri Oct 05 10:25:38 2001 Page 3

NYC-WTC_000087359

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NYC-WTC_000087359Source: NYC Law Department, mirrored locally

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