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GCMS calibration table for TCLP analysis, Nov 2 2001

Machine-extracted title · confidence 100%

Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.

NYC-WTC_000067979–000067989

Folder label: “GCMS Scan X 10/10/01 An 11/1/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\LB.D Vial: 2 Acq On : 31 Oct 2001 5:05 pm Operator: 209 GALOS San^le : 10/10 Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.37 ug/1 219745 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone74-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 2-PropanoBf 2-methyl- 74 C4H1O0 000075-65-0 12 3 3-Hydro: -2-pentanone 102 C5H10O2 003142-66-3 9 4 Acetone 58 C3H6O 000067-64-1 9 Miundance Scan 289 (7.695 min): LB.D (-) m/z 42.95 100.00%

59 5000 101 7.40 7.60 7.80 8.00 ............... .............. ........... m/z 59.05 55.23% nZz-> 10 20 M 50 60 70 80 90 100 110 Abundance #3245:2-Pentanone, 4-hydroxy-4-m8thyl- 40

5000 59 —I I , I I I I , 1 I rr-pT 11.11 7.40 7.60 7.80 8.00

31 83 101 .........................I I 73 n-* TiZz-> 10 20 30 40 50 60 7080 90 100 110 Abundance #62575:2-Propanol. 2-tnethyl-

• ■ I • ■ • ■ I ■ • • • I ■ ' ^1' ' 7.40 7.60 7.80 8.00 5000 m/z 58.05 17.11% 31

L 41 ^5 OR I, . I . j, . , , )l, ' I ' ' ' ‘ 1 ' ' ' ' I ‘ ' I ' ' ' ‘ I ' ' ' ‘ I Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 58 7.40 7.60 7.80 8.00 ra/z 41.05 8.28% 5000- 45 15 I ‘ ‘ \.. II.. ' I ' ' ' ‘ 1 ' ' ' ‘ 1 nn I, 66 73 84 102 T)fe-> 10 20 30 40 50 60 70 80 90 100 110 ' '7.40' '7.^ 7.^ ' 8.00

LB.D NP103001.M Fri Nov 02 17:17:24 2001 Page 3

N YC-Wf C_000067987

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NYC-WTC_000067987Source: NYC Law Department, mirrored locally

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