GCMS calibration table for TCLP analysis, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\LBB.D Vial: 27 Acq On 19 Dec 2001 4:37 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.67 0.66 ug/1 279705 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, hydroxy-4-methyl- 116 C6H12O2 000123-42-2 83 2 Acetic acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 28 3 Morpholine, 4-methyl- 101 C5H11NO 000109-02-4 12 4 CH2=CHCH2C (O)OCH3 100 C5H802 003724-55-8 10 Abundance / Scan 286 (7.672 min): LBB.D (-) i m/ z 42 . ( 100.00% 413

5000 69

101 7.40 7.60 7.808.00 284 +1++ IT ' T 67 83 ! । qu94'. TTTmmg m/z 59.05 47.90% miz-2 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 FTTnr 59 ___ 7.40 _ 7.60 7.80 8.00 27 101 m/ z 58.05 17.70% 49 83 COT । r', t T T t- t -r- > p- i ■ ■ • ■ i 1 ' । ■ i ' 1 TIp' ‘ ‘ I 1' 1 Trp m/z->____ _ 10 20 30 40 50 60 70 80 90 100 110 Abundance uod. 1,1 -din eti 43 frrMrrTTTT f r ' r । T 7.40 7.60 7.80 8.00 5000 57 m/z 100.95 17.07% 101 15 27 ■!

m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63448: Morpholine, 4-methyl- 43 7.40 7.60 7.80 8.00 m/z 41.05 7.61% 5000

m/z--> T-r~r-r~n-i T 10 20 T T CtO") 30 40 56 — # II 50 60 70 । 71

80 82 87 93 90 101

100 110 .. N —iTT T TTTT । । ' TTTT । i । । j । । TT : 7.40 7.60 7.80 8.00

LBB.D GCMS1126.M Wed Jan 02 12:10:34 2002 Page 3

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