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GCMS analysis results, sample AD25602, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25602 conducted on November 28, 2001, noting unknown compounds.

NYC-WTC_000069778–000069789

Folder label: “GCMS Scan X 10/27/01 An 11/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25602.D Vial: 14 Acq On : 17 Nov 2001 3:43 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.75 ug/1 129057 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanoner 100 C6H12O 000591-78-6 91 2 Methyl l^obutyl Ketone 100 C6H12O 000108-10-1 58 3 Oxir^, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 56

.u 4 2-Pe^ene, 2-methoxy-_______ ___________ 100 C6H12O 061142-47-0 41 Mjundance Scan 150 (6.419 min): 2S«)2.D(-) m/z 42.95 100.00%! 4|3

58 5000

71 6.00 6.20 6.40 6.60 6.80 38 1 51 Wz 58.05 61.80% I““I nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63387:2-Hexanone 4|3

58 5000 — y............ 6.00 6S_6^25£ZS^_. 100 Wz 57.00 18.20% +TrrTTrrrTTtl+T 71 85 TTtt+p+ Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1526: Methyl Isobutyl Ketone 43

6.00'' 6.40 6.60 6.80 5000 58 m/z41.0516.60% 27 85 100 53 67 yTTTTjTrT^TTrTyrrrr^TTT^TTTTjrrr^ TTJTTTTyr 'l"■'l""l' Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 4(3 6.00 6.20 6.40 6.60 6.80 58 m/z 100.05 12.76% A 5000 71

30 66 Tn.TTTTTTrrHT.7TTTTp+ tt/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

25602.D NP103001.M Tue Nov 27 09:41:40 2001 Page 1

NYC-WTC_000069786

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NYC-WTC_000069786Source: NYC Law Department, mirrored locally

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