GCMS analysis results for sample AD25732, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25732.D Vial: 17 Acq On : 17 Nov 2001 6:38 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.44 0.45 ug/1 88075 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 tative ID MW MolForm CAS# Qual

1 2’HexanonoY 100 C6H12O 000591-78-6 90 2 Methyl I/obutyl Ketone 100 C6H12O 000108-10-1 58 3 2-Hexa^ne, 4-hydroxy-5-methyl-3-pr 172 C10H20O2 061141-74-0 45 4 Oxirapfe, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 45 Abundance Scan 152 (6.436 min): 25732.D (-) TWz 42.95 100.00% 4(3

58 5000

71 85 100 6.00 6.20 6.40 6.60 6.80 53 ....... m/z 58.05 57.21% p/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 \bundance #63387:2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 100 "mT^ 57.00 16.42%

I'''' I'''' I +p+ . ...... 1'1 TTp-rrrjI-rTTp-rTip-rrT]^^ " I'" ' '' I'''' I ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63351: Methyl Isobutyl Ketone 4(3

6.00 6,20 6.40 6.60 6.80 5000 m/z 41.00 15.71% 58 27 85 100 I’'"I " I ' ' ' rj +t i?2,i........................... I..,,,..... Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4|3 6.00 6.20 6.40 6.60 6.80 m/z 100.00 12.49% A 5000 58 27 72 .1 85 100 n TpTT-rpHTTrpTnnyrTTTjTTTTpTTTyrTTrf^^ ■nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

25732.D NP103001.M Wed Nov 28 14:21:15 2001 Page 1

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