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GCMS analysis results for sample AD24486, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24486 identifying unknown compounds on November 13, 2001.

NYC-WTC_000068799–000068810

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0201\24486.D Vial: 25 Acq On 3 Nov 2001 2:20 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.45 ug/1 66872 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone/ 100 C6H12O 000591-78-6 86 2 2-Hexanoi3/ 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 3 Methyl^^sobutyl Ketone 100 C6H12O 000108-10-1 53 4 Oxirarfe, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 50 Abundance Scan 150 (6.418 min): 24486.D (-) m7z 42795 100.00% 43

58 5000

6.00 6.20 6.40 6.60 6.80 ....... , , , , ,l,l| ” - 71 m/ z 58.05 58.53% Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6-80'' m/z 41.00 12.95% 27 71 85 100 ........ l'......... 'I ......... ■I............ TTfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance ;#11968; 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.00 6.20 6.40 6.60 6.80 5000 29 m/z 56.95 12761%

71 100 ' I ' ' ' ' I ' ' ' ' I I J. I 85 ' I ' ' ' ' I ' I 140 Tt/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63354: Methyl Isobutyl Ketone 43 6.00 6.20 6.40 6.60 6.80 m/z 85.05 10.95% yTT 58

...................... I,( I 85 67....... , , ,1, 100 ,I ,,,,,,, ........ . , , m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80

24486.D NP103001.M Fri Nov 09 12:39:56 2001 Page 1

NYC-WTC_000068807

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NYC-WTC_000068807Source: NYC Law Department, mirrored locally

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