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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088124
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCTO 901\23262.D Vial: 8 Acq On 9 Oct 2001 8:12 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *************************************************** ****************** Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

29.51 0.63 ug/1 130038 Chrysene-dl2 33.13

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentan^arboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 38 2 Cyclopentaprecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 38 3 l-Hexeney/2-methyl- 98 C7H14 006094-02-6 27 4 Cyclobutanone, 3,3-dimethyl- 98 C6H10O 001192-33-2 27 4bundance Scan 2665 (29.505 min): 23262.D (-) m/z 56.00- 100.00% 53

5000 41 73 ................... .................................. 9*57 -.101 129 239 I 29.20 29.40 29.60 29.80 .[| .87.I.I 11|5 I 1431571711851992p [ 1_______ 312 TfrV'lS-pVTTyT-iMYr-iS-ry'rTTTYrTVTph-i-rp-r-iS-p-i-rTl-i^^p-rrryiTT-T-p-rhT-p m/z57.00 42.68% Wz~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 * Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-, cis- c:

553 29.20 29.40 29.60 29.80 m/z 41.05 k 36.70% 30 ,1 , [ ' ' ' ' ( ' ' * ' I ' ' ' ' I ' ' ' ' I 1 r. . I . . . I I .... I . i .1 I .. I ■ I .... I .... I I ... I .. I . I Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- 55

29.20 29.40 29.60 29.80 5000 m/z 43.00 36.30%

30 100 129

■n/z-> 20 ,1 . 40 Ty-rm-p-r 60 yr 100 80 120 140 160 180 200 220 I'''' I'''' I'''' I'''' I'''' I' ''' I 240 260 280 300 Abundance #63261:1-Hexene, 2-methyl- 5 29.20 29.40 29.60 29.80 m/z 73.00 30714% 41 5000- 27

1 98 T I'''' I'''' I I'''' I'''' I'''' I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23262.D NP091101.M Thu Oct 11 10:47:59 2001 Page 3

NYC-WTC_000088124

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NYC-WTC_000088124Source: NYC Law Department, mirrored locally

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