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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088125
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23262.D Vial: 8 Acq On 9 Oct 2001 8:12 pm Operator; 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butyl tetradecanoate (myristat Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 31.64 0.52 ug/1 106960 Chrysene-dl2 33.13 it# of 5 Tentative ID MW MolForm CAS# Qua! .^Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 86 2 Oxirane, 2,3-bis(1-methylethyl)-, t 128 C8H16O 054644-32-5 32 3 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 32 4 Octadecanoic acid, 2-methylpropyl e 340.C22H44O2 _____ 000646-13-9 30 Abundance Scan 2898 (31.644 min): 23262. D (-) m/z 55.95 100.00% 5|6

553 4 73 129 285 m, ■n/z-> Abundance I''' ‘ I' 20 40 JjUL. 60 .[ .. 157 , ■'^5 ■.'i . I ’l 'l 1 I I j. . I 111.11 ’l

80 100 120 140 160 180 200 220 240 260 280 300 320 340 #40186: Butyl tetradecanoate (myristate) xxu 340 rrfn m/z 31.40 31.60 31.80 32.00 57.00 5^765%

5|B

5000 229 31.40 31.60 31.80 32.00

■n/z-> Abundance 20 40 60 u 73

r' 129 211

I '' '' I ' ' ' ' 1 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #5067; Oxirane, 2,3-bis(1-methylethyl)-, trans­ 284 m/z: 43.00 46.75%

55 41 31.40 31.60 31.80 32.00 5000 m/z; 41.05 36.20%

■n/z-> *\bundance 20 40 u60 , 73

80 113128 I'''' I'''' 100 120 140 160 180 200 220 240 260 280 300 320 340 #28775: Pentadecane, 8-methylene- 5|S 31.40 31,60 31.80 32.00 mZz 73700 32.32%

5000

27 84 I I'''' I'' T I . I ' ' ' ' 1 Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23262.D NP091101.M Thu Oct 11 10:48:02 2001 Page 4

NYC-WTC_000088125

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NYC-WTC_000088125Source: NYC Law Department, mirrored locally

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