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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088126
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23262.D Vial: 8 Acq On : 9 Oct 2001 8:12 pm Operator: 209 GALOS Sample : g c/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L **************** * * *************************************************** Peak Number 5 Octadecane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.74 0.70 ug/1 144031 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91V. 2 Tetracosane 338 C24H50 000646-31-1 90 / 3 Pentadecane 212 C15H32 000629-62-9 86^ 4 Dodecane, 1-iodo- 296 C12H25I 004292-19-7 80 Abundance Scan 2908 (31.736 min): 23262.D (-) m/z 56.95 100.00% 517 43 71

5000 85

31.40 31 60 31.80 32.00 TrYrrrlY’-riHYmT-jhn-TVp-rTTpTn-TyrTTTpTnT-pTT-rpTnn-pnTn-p^^ m/z 71.00 70.07% n/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 “Kbundance #71559: Octadecane 43 57

71 5000 . ......... /yy 85 31.40 31.60 31.80 32.00 m/z 43.00 67.79% T 1^127141155169183 226 254 r ''' i'''' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 31.40 31.60 31.80 32.00 5000 85 m/ Z 85.05 48.87%

99 Il I ll 155169183197 294 338 I' '' ' I"' '' I' ‘' I'' '' i' 'I''''' I'' '' I' I'''' i I''''I I ” "I' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #70278: Pentadecane , A /, V , 43 57 31.40 31.60 31.80 32.00 m/z 41.05 25.35% 71 5000 85

113127141155169 212 ' I ‘' I ‘ j PI . I I I I' I > I '< I I > I I I I '''' I'''' I'''' I'''' I 4^ •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23262.D NP091101.M Thu Oct 11 10:48:04 2001 Page 5

NYC-WTC_000088126

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NYC-WTC_000088126Source: NYC Law Department, mirrored locally

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