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GC/MS analysis results for sample AD23260, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23260 conducted on October 12, 2001.

NYC-WTC_000088079–000088097

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088093
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0901\23260.D Vial: 6 Acq On : , 9 Oct 2001 6:15 pm Operator: 209 GALOS Sample : g c/ms unknown Inst : GC/MS 209 Mise ■ Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Octadecane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.61 0.87 ug/1 166335 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 0O0593-45-3 93\ 2 Heptadecane, 8-methyl- 254 C18H38 013287-23-5 91 / 3 Tetracosane 338 C24H50 000646-31-1 90 / 4 Heneicosane 296 C21H44 000629-94-7 '907 Abundance Scan 3221 (34.610 min): 23260. D (-) m/z 57.00 100.00% 57 71 43 85 553

.1 1, j. J T\|^\27141155169183 207 224 256 281 34.20 34.40 34.60 34.80 35.00 TT-p-T^rp-THq^TT-H^yTn+T-j-rrrrp-TT'Vp-thT-f'YTTr^ ' I'''' I'''' I' "mTz 71.05 71716% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71559: Octadecane 43 5(7

71 552 85 34.20 34.40 34.60 34.80 35.00 ■mTz 41705 61.10% 113127141155169183 226 254 I ' I ' ' ' ' I ' ' f' ' ' I ' ' I ' ‘ ' I p-i-TTp-rTT-j- ’ I ■P" b/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #34816: Heptadecane, 8-methyl- 57 71

85 34.20 34.40 34.60 34.80 35.00 5000 m/z 85.05 52.22% 126

•n/z-> 40 60 99 J i ' I ' ' ' 154

I ' ' I I '' ' ' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 224 254 ' I " " I r. . I I I ' ' ' ' I

Abundance #73543: Tetracosane 43 57 34.20 34.40 34.60 34.80 35.00 71 "mTz 55.00 25.34%

5000 85

•nfe~> 40 60 ''' I 80 99 J \]3127 ' I ' " ' I " " I ' •I ' 155169183197 ' I’l ' '- I I 100 120 140 160 180 200 220 240 260 280 300 320 340 I'''' I'''' I'''' I'' ‘' I 294 338 I''' 'I' 1 ' ' ' Jk 34.20 34.40 34.60 34.80 35.00

23260.D NP091101.M Thu Oct 11 10:44:05 2001- Page 8

NYC-WTC20b0088093

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NYC-WTC_000088093Source: NYC Law Department, mirrored locally

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