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GC/MS analysis results for sample AD23260, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23260 conducted on October 12, 2001.

NYC-WTC_000088079–000088097

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088094
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23260.D Vial; 6 Acq On : 9 Oct 2001 6:15 pm Operator; 2 09 G7VLOS Sample : g c/ms unknown Inst : GC/MS 209 Mise - Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Octadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 35.50 1.04 ug/1 158129 Perylene-dl2 37.24 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91' 2 Pentacosane 352 C25H52 000629-99-2 91 3 Tricosane 324 C23H48 000638-67-5 91 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91' Abundance Scan 3318 (35.501 min): 23260.D (-) m/z 57.00 100.00% 57 71 A 43 85

J L,, i iJ ^j^‘'?^141155169183197 35.20 35.40 35.60 35.80 253 281 YT, it«l I I fl I I'I I 11'I n-i 11 I ' ' ' I ' ' ' ' I ' m/z TITTo 74.16% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane 57 43 71

85 5000 35.20 35.40 35.60 35.80 tuTz 43.00 68.31% 99 J J■'41155 ................. 224 . .254 'I ' 'I'I ' 111 ■ I' I ' ' ' I I I ' ' ' ' t ' ' ' ! ' ' ' ' I ' ' ' ' I p-r-rrp-TT-p- n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73718; Pentacosane 3 57

71 J 35.20 35.40 35.60 35.80 'rrr m/z 85.05 52.05% 85

j II 1 ■’■’3127141155169183197211225 I I I II I I T I I I I I I 1 I I I I I I (' I I I 'i I I f erp ' ' ' I I ’ I I I I I I I I '' I' I ' ' ' ' I ' ' ' ' I ' ' ' ' I •n/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 43 57 ■ 35.20 35.40 35.60 35.80 m/z 41.05 26.45% 71 5000 85

183197211225 296 324 -p « . . I I I TCI III I I . ' I'' ' I' ''' I ' p-m-p-m-j -r-rp-r-n-p-Tn Tl/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 35.20 35.40 35.60 35.80

23260.D NP091101.M Thu Oct 11 10-.44; 07 2001 Page 9

NYC-WTC_06b08‘80‘94

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NYC-WTC_000088094Source: NYC Law Department, mirrored locally

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