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GC/MS analysis results for sample AD23262, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088127
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23262.D Vial; 8 Acq On : 9 Oct 2001 8:12 pm Operator; 209 GALOS Sample : g c/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NPO91101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Tetracosane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 32.74 0.74 ug/1 151334 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 9IK 2 Tricosane 324 C23H48 000638-67-5 91 \ 3 Heptadecane 240 C17H36 000629-78-7 91 / 4 Hexacosane 366 C26H54 000630-01-3 90/ Abundance Scan 3017 (32.737 min): 23262.D (-) m/z 57700 100.00%

43 57 71 J 5000 85 , J, , , I , I , , , 11-5 32.40 32.60 32.80 33.00 T-ry-m-rp- m/z71.00 75.52% Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

552 85 I 3Z40 32.60 32.80 33.00 m/z43.05 67.28% l| 1/127 155169183197 I I pTHT-pTTnyrTTryrrTTy 294 338 '' I' I ' ' ' ' I I' ' '' I ' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #46165: Tricosane 43 57

71 32.40 32.60 32.80 33.00 552 m/z 75/05 47.19% 85

T pi 155169183197211 253 1 -f-p-rrTy-r 297 324 I' " ‘ I ‘' I'''' I ' Ti/z-> 40 60 80 100 120 140 160 180 .200 220 240 260 280 300 320 340 Abundance #71193; Heptadecane 57 32.40 32.60 32.80 33.00 in/z 41.05 25.53% 71 5000 85

99 J ^^■’27141155169 210 240 I ' ' ' ' I ”' ' ' I ' I r I I ' ' ' ' I'' ' ' ' I ' ‘ I I I I ' ' I I ' ' ' ' I ' TTT-|T-rTTpT-rTyTTTTpT-rT-p-r^^ \ /—aA AZ'—Aza?^^\a a T-rp-r ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

23262.D NP091101.M Thu Oct 11 10:48:06 2001 Page 6

NYC-WTC_000088127

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NYC-WTC_000088127Source: NYC Law Department, mirrored locally

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