GCMS analysis comments for sample AD28693, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DECO4 01\28693.D vial: 8 Acq On 4 Dec 2001 7:12 pm Operator: 209 ___ GALOS Sample gc/ms 11/24 Inst : GC/MS 209 MisC : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentanecarboxylic acid, 2 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.43 4.77 ug/1 919694 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentanecarbory lie acid, 2-amin 129 C6H11NO21 040482-05-1 35 2 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 3 Cycloheptylamine 113 C7H15N 005452-35-7 27 4 Cyclobutane,/I,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 Abundance 7 Scan 2657 (29.434 min): 28693D (-) m/z 56.00 100.00% 55

5000 41 73 129 239 2|7 TT 1 i — —IT 15 [ 143157171185199213 | 1 312 29.20 29.40 29.60 29.80 — HTTt TIT T r| n TIT TIII i'i TTTTT .. 4 m/z 56.95 49.05% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans- 55

—- — — ----- 5000 29.20 29.40 29.60 29.80 m/z 43.00 40.32%

Im, 30 70 84 100 129 i r" ■ i ■ ■ MA i ■ • ■ ■ i mz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1354:1-Hexene, 2-methyl- 55

41 29.20 29.40 29.60 29.80 5000 m/ z 41.05 39.30%

27 170 m/z—> 20 l 40 60 98 I 1 I 1 . . .-| 1’’’ TT’T : . j I I . I | . I I I | I I . . | I > I b | I I I I | . < I r | . . < < | 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #2793: Cycloheptylamine 55 29.20 29.40 29.60 29.80 m/z 55.00 30.11% 5000

70

m/z-> 20 l LeA 30

40 60 80 113 TTTT TT 100 120 140 160 180 200 220 240 260 280 300 I" " I i ■ ■ ■ ■ i ■ ■ ■ ■ i T-l-|-t-| .T-) . I’I I T11" 29.20 29.40 29.60 29.80

28693.D GCMS1126.M Thu Dec 06 15:19:35 2001 Page 1

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