GCMS analysis comments for sample AD28693, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28693.D Vial: 8 Acq On 4 Dec 2001 7:12 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C: \HPCHEM\1\METHODS\GCMS1126 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Nonadecane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 29.55 0.82 ug/1 157669 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qu 1 Nonadecane 268 C19H40 000629-92-5 91 2 Heptadecane 240 C17H36 000629-78-7/91 3 Tetradecane 198 C14H30 000629-59-4 91 4 Octadecane ____________________ 254 C18H38 _____ 000593-45-3 91 Abundance Scan 2670 (29.554 min): 28693.D (-) m/z 57.00 100.00% • 57 43 71

5000 85

99 TTT TT‘**0——uTr 29.20 29.40 29.60 29.80

m/z-> —HUI 40 60 l 113 127 141 155 169 183 197 211 225 80 100 i i T. । . f. . .^ । 1 120 140 160 180 239 TTT i i i-1 ri ■> । । r । i 11 । । । । । i । 200 220 240 260 m/z 43.00 79.63% Abundance #71949: Nonadecane 57

5000 71

85 1 i 1 ' JWA_ 29.20 29.40 29.60 29.80 99 m/z 71.00 68.34% II" 1’’ —T l , 113127 141,155 169 183 -224268 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #32063: Heptadecane 57 71 T TT ■ . . ■ j TTf 85 29.20 29.40 29.60 29.80 5000 m/z 85.00 45.50% 99 113 127 141 I I — || 240 ■ • i • T’U L 196 i ' ' ' ■ i ■ 1 • ■ i ■ ■ ■ ■ I ' 1 1 1 I 1 ' 1 1 I 1 —T '' m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 - Abundance #69662: Tetradecane 57 71 29.20 29.40 29.60 29.80 m/z 41.00 25.25% 85 5000

m/z-> ' k I ' ' 40 — 60 80 2113,127 141154 180 200 220 ’ 240 260 100 120 140 160 198

29.20 29.40 29.60 29.80

28693.D GCMS1126.M Thu Dec 06 15:19:37 2001 Page 2

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