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GC/MS analysis results for sample AD23501, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.

NYC-WTC_000088853–000088879

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088868
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT16O1\235O1.D Vial: 9 Acq On : 16 Oct 2001 10:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ***************** * * ************************************************** Peak Number 9 Nonadecane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.70 1.87 ug/1 209237 Chrysene-di2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qua! 1 Nonadecane 268 C19H40 . 000629-92-5 9i 2 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6, 91 3 Tetracosane 338 C24H50' 000646-31-1 90 4 Pentacosane ___________________________ 352 C25H52 000629-99-2 87 Abundance Scan 2795 (30,697 min): 23501 ,D (-) m/z SYTOO 100.00% 57 '43 71

5000 85

J.Vr.. ■n/z-> Abundance MU 40 u 60 99 i lj T.^?71411^169183197 225____________________ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #37469: Nonadecane 30.40 30,60 30,80 31,00 jn/z 71.00 71.77% (1 43 71

5000 85 JL I ' ' ' 30,40 30,60 30,80 31,00 'l

m/z 43.05 71.48% 99 I '' I' J 113127 183197 I' '' ' I '' ’' I' ''' I'''' I 268 I'''' I'''' I'''' I ■p" n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl-

71 V T ' 30,40 30,60 30,80 31,00 5000 85 ■m/z 85705 49771%

I, 183 211 268 296 I rm-| I I I I I r. i । । nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane I ' ' ' ' I 43 57 —-30;40-30,60 -30:80--31,00 71 :m/z" 41.05- 29.51% 5000- 85

,11 ■! Jl. n^YTTYTpVrTpT-TVp-rTTyVTTTY ’'TTT^^ 294~ 338 1 T*r p. 1*1*11"!I ?■[ , i~r r| 17 ? I* I'''' I I''' ‘ I' I''' ' I,' Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30,40 30,60 30,80 31,00

23501.D NP091101.M Thu Oct 18 10:21:38 2001 Page 9

NYC-WTC_000088868

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NYC-WTC_000088868Source: NYC Law Department, mirrored locally

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