GCMS analysis comments for sample AD28694, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28694.D Vial: 5 Acq On 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************** Peak Number 4 Nonadecane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.63 0.52 ug/1 128225 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qu. 1 Nonadecane 268 C19H40 000629-92-5 1 2 Tetracosane 338 C24H50 000646-31-1 1 3 Octacosane 394 C28H58 000630-02-4 1 4 Docosane 310 C22H46 000629-97-0 1 Abundance Scan 2787 (30.627 min): 28694.D (-) m/z 57.00 100.00% 57

85 5000 4 -T P P r mlz-> m .................... ............... ........ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 30.20 30.40 30.60 30.80 31.00 m/z43.05 79.22% Abundance #37469: Nonadecane 57

85 5000 ff T"T Tfrrri 30.20 30.40 30.60 30.80 31.00 m/z 71.00 75.63% 1 J 113 268 - TTTTT’T183 ! . . . 1 । , , , , । , . , , TTTTT I "1—000000 mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73543: Tetracosane 57 =r Prem fr / rPA PPrr r 30.20 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 50.73%

111 JUL T‘ 1I’TIII’ 113.155 TT j.. f. r..183 ___ |I«... I.... I.... |.... |. T29 ‘14—01—T0338—ITr r mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74211: Octacosane TPrTTTPr { ets — 43 30.20 30.40 30.60 30.80 31.00 m/z 41.00 31.06% 71 5000

9127155 183 211........... 364. MYM , “WAAN Tn-p-TT T‘"""ETTTTTTTTT‘‘‘‘I‘T‘. ।. j. ■ i r 11 .k. ।. 1111111 > 111111 > 11 TIUI0""00—00‘"7T m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 30'20 30.40 30.60 30.80 31.00

28694.D GCMS1126.M Thu Dec 06 15:34:04 2001 Page 4

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