GCMS analysis comments for sample AD28664, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\DEC 0401\28664.D Vial: 18 Acq On 5 Dec 2001 4:58 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Nonadecane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

29.55 0.60 ug/1 137551 Chrysene-dl2 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonadecane 268 C19H40 000629-92-5 2 Heneicosane 296 C21H44 000629-94-7 3 Heptadecane 240 C17H36 000629-78-7 4 Tetradecane 198 C14H30 ____ 000629-59-4 Abundance Scan 2670 (29.554 min): 28664.D (-) m/ z 57.00 100.00%

L 57 43 71 5000 85 "It . I I J l l . . j . . 1 1 1 . . . . 1 . 99 in 29.20 29.40 29.60 29.80

miz-> • TTT 40 +ul60— .804, . 100 a . 17 141,155 169,183 .............. —........ m/ z 120 140 160 180 200 220 240 260 280 300 63.70% Abundance #71949: Nonadecane 57 71 5000 85 ■ i 1 ■ 29.20 29.40 29.60 29.80 A 99 m/z 7 .00 61.24%

mz—s 40 60 80 l . 113127 141,155 169,183 ..... .......... ......... 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 : 85 T-p-r A 29.20 29.40 29.60 29.80 5000 m/z 85.00 46.42% 99 : 1 113 127 141 155 268 296 111" ‘TTu—u—u.rrm‘—‘——uu1—‘TTr)m m/z-> Abundance 40 60__ 80 100 _ 120 140 160 180 200 220 240 260 280 300 . ......... 57 ' #32063: Heptadecane _ LU.A I ■ . _ 29.20 29.40 29.60 29.80 71 m/z 41.00 33.72% 85 5000 99

m/z-> TTITTTTTT 40 60 80 113 127141 , 196 240 100 120 140 160 180 200 220 240 260 280 300 TIP — PPPT 29.20 29.40 29.60 29.80

28664.D GCMS1126.M Fri Dec 07 15:53:44 2001 Page 2

NYC-WTC_000035125