GCMS analysis comments for sample AD28664, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC0401\28664.D Vial: 18 Acq On : 5 Dec 2001 4:58 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Acetic acid, octadecyl ester Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

29.68 0.66 ug/1 151351 Chrysene-dl2 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 2 1-Nonadecanol 284 C19H40O 001454-84-8 81 3 1-Docosene 308 C22H44 001599-67-3 60 4 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 60 Abundance Scan 2684 (29.682 min): 28664.D (-) m/z 43.05 100.00% 43

57 83 97 5000 AA29.40 29.60 29.80 30.00 125 140153 168 i1 ■ ■' 1'11' I'1'1 T’T < • 111111।।11.. m/ z 55.00 57.46% miz-2 40 60__ 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #73048: Acetic acid, octadecyl ester 43

5000 — TITT TTT m-, । T 61 83 97 29.40 29.60 20 30 30.00 111 _ m/z 83.05 53.48% TI‘ — 1 1125139 |T i l i il . । i ■ ■ • ■ i 224 252 i11 ' ' I '1 ‘11 i1" 11 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 55 69 83 09 97 440236; 1-Nonadecanol

A29.40 29.60 29.80 30.00 m/z ,97.05 48.99% 5000 111 42 125 I. . —........ ... 238 ... ' 40 " 60 " 80 100 120 140 160 180 200 220 240 260 280 300 miz-2 Abundance #72943: 1-Docosene 55 29.40 29.60 29.80 30.00 m/z 57.00 48.79% 83 97 5000 70 111 42 125

m/z-> X ‘II’rTTTT 40 60 80 , |, 139_________________________ 308 TTT TTTIrr | I ! . I | I I I . | I ! I . | I f I I | I I I I | I ) I I | i i i I | i i I I | I I I

100 120 140 160 180 200 220 240 260 280 300 — A........... 29.40 29.60 29.80 30.00

28664.D GCMS1126.M Fri Dec 07 15:53:49 2001 Page 3

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