GCMS blank analysis for sample AD28662, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC 040128662.D Vial: 15 Acq On 5 Dec 2001 2:02 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Acetic acid, octadecyl ester Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 29.68 0.54 ug/1 115855 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, octadecyl ester 312 C20H40O21 000822-23-1/87) 2 17-Pentatriacontene 491 C35H70 006971-40-0 58 3 Acetic acid, dodecyl ester 228 C14H28021 000112-66-3 50 4 1-Octadecanol 270 C18H380 000112-92-5 49 Abundance Scan 2684 (29.684 min): 28662.D (-) m/z 43.05 100.00% 43

5000 83

L 1139 111 224 ............. .................... — A..... 29.40 29.60 29.80 30.00 ■ ■ i ' m/z 83.05 47.29% miz-> 50 100 150 200 250 300 350 400 450 Abundance #73048: Acetic acid, octadecyl ester 43

5000 83 29.40 29.60 29.80 30.00 I 111 m/z 97.05 46.26% hi | 1139 .... 224 252 ................... miz-> 'sb 100 150 200 250 300 350 400 450 Abundance 43 #58705:17-Pentatriacontene

A.. . 29.40 29.60 29.80 30.00 5000 83 m/z 56.95 45.79% , 111 __ 462 490 ■ ‘i1 ■ i ' ' ■ ■ i ' ■ ■ ' i mfe-> Abundance 50

43 100 150 200 250 300 1350— #29639: Acetic acid, dodecyl ester 400 450 L — I ' 1 — — 29.40 29.60 29.80 30.00 m/z 41.05 44.03% 5000- 83

111 140 168 1’ — 4 ■l ■ 228..................................................... t-i i f i TPPP — । ri m/z—> 50 100 150 200 250 300 350 400 450 29.40 29.60 29.80 30.00

28662.D GCMS1126.M Thu Dec 06 13:20:06 2001 Page 3

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