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GC/MS analysis results for sample AD23320, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088225
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS, 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Acetic acid, octadecyl ester Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 31.86 0.41 ug/1 45396 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 91 2^1-Eicosanol 298 C20H42O 000629-96-9 76 3 1-Octadecanol 270 C18H38O 000112-92-5 62 4 17-Pentatriacontene 491 C35H70 006971-40-0 58 Abundance Scan 2922 (31.862 min): 23320.D (-) m/z 43.05 100.00% 43

61 83 5000 97 111 125 31.60 31.80 32.00 32.20 T 139 HJILJ ..........207 ............... m/z 83.05 59.95% ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #73048: Acetic acid, octadecyl ester 43

61 83 97 Ba 31.60 31,80 32.00 32.20 m/z 61.05 55757% 1 I 139 224 252 ' ' I' ' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72722:1-Eicosanol 57 83 69 97 31.60 31.80 32.00 32.20 5000 111 m/z 57700 53.48% fl 125 139 I 167 Ti/z-> 40 60 80 -BUB 280 100 120 140 160 180 200 220 240 260 280 / \ Abundance #72028:1-Octadecanol 57 83 31.60 31.80 32.00 32.20 69 97 m/z 55.00 49.56% 5000 111

125 I 140153 224 r-r-r T ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 31.60 31.80 32.00 32.20

23320.D NP091101.M Mon Oct 15 09:53:56 2001 Page 12

NYC-WTC_000088225

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NYC-WTC_000088225Source: NYC Law Department, mirrored locally

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