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GC/MS analysis results for sample AD23270, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.

NYC-WTC_000088346–000088371

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088359
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23270.D Vial: 18 Acq On : 12 Oct 2001 6:44 pm Operator: 209 GTILOS Sample : gc/ms unknown Inst : GC/MS 209 Mise - Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Acetic acid, octadecyl ester Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 29.76 0.55 ug/1 59043 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 91 4-Tetradecanol 214 C14H30O 001653-33-4 81 3 1-Eicosanol 298 C20H42O 000629-96-9 76 4 1-Octadecanol 270 C18H38O 000112-92-5 76 Abundance Scan 2692 (29.757 min): 23270.D (-) m/z 4^/95 100.00% 43

57 69 97 5000 111 139 207 JAA™ 2940 29.60 29.80 30.00_____ m/z 83.05 62.86% n/z-> Abundance 40 60 80 100 120 140 160 180 200 #73048; Acetic acid, octadecyl ester 220 240 260 280 ft 43

5000 61 83 97 JUA I ' ' ' ' I ' ' ' ‘ I 29.40 29.60 29.80 30.00 m/z 57.00 56.29% Illi III II ,1, '*^1^ 224 252 Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 ft Abundance #26420: 4-Tetradecanol 43 57 83 kA ' ” 'I I" 97 29.40 29.60 29.80 30.00 5000 m/z 60795 53.29% 70 111 ft 125 I...... 166... 196............. ■ -nZz-> 40 60 80 100I 120 140 160 180 200 220 240 260 280 Abundance #72722:1-Eicosanol ' ' ■ I 57 83 29.40 29.60 29.80 30.00 69 97 m/z 69710 50.34% 111 ft 5000

I Tl/Z-> ' ‘ I' 40 60 80 100 120 125

140 167 160 180 200 220 240 260 280 A Iki 29,40 29.60 29.80 30.00

23270.D NP091101.M Mon Oct 15 09:33:42 2001 Page 7

NYC-WTC_000088359

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NYC-WTC_000088359Source: NYC Law Department, mirrored locally

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