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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088226
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On ; 12 Oct 2001 1:51 pm Operator; 209 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 13 Octadecane Concentration Rank 4 R.T. EstConc Area Relative to .ISTD R.T. 32.73 4.36 ug/1 479822 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecane 254 C18H38 000593-45-3 91 2 Heneicosane 296 C21H44 000629-94-7 9i> 3 Heptadecane 240 C17H36 000629-78-7 91 4 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91' ftbundance Scan 3017 (32,734 min): 23320,D (-) m/z 57.00 100.00% 5/

252 85

4’ I TlZz-> 0 40 J 60 169 197 '' I' " • I 224239 267 352 I • " • I««• • I • • • • 1'' • • I« " ' I " ' • I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32,40 32,60 32,80 33,00 m/z 71.00 71.12% Abundance #71561: Octadecane 57

85 253 32,40 32,60 32,80 33,00 m/z4370564777% 224 2^ I' 'I' I... I ' I f' I''' I (I' I"'' I' *" r rpT-rrp-rTVy- I " '' r ' " I' " ' I " '' I Tl/Z-> 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #42201: Heneicosane c7

'' 'I 85 32.40 32,60 32.80 33,00 5000 m/z 85.05 J 49.11%

268 296 r' ’ ' I I' ''' i '''' I Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance c7 #32063: Heptadecane / kT 32,40 32,60 32,80 33,00 m/z 55.00 23.91% 85 5000

I 113 141 240 196 ‘' I ' ' p-TTTp-rrrp I' " ‘ I' " ‘ I " '' I TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32,40 32,60 32,80 33,00

23320.D NP091101.M Mon Oct 15 09:53:59 2001 Page 13

NYC-WTC_000088226

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NYC-WTC_000088226Source: NYC Law Department, mirrored locally

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