GCMS analysis comments for sample AD28664, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC04 01\28664.D Vial: 18 Acq On 5 Dec 2001 4:58 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Heptadecane, 2,6,10,15-tetrame Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

30.63 0.54 ug/1 123275 Chrysene-dl2 33.04

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 8 7 2 Heneicosane 296 C21H44 000629-94-7 8 7 3 Dotriacontane 451 C32H66 000544-85-4 8 7) 4 Nonadecane 268 C19H40 000629-92-5 8 Abundance Scan 2787 (30.628 min):28664.D (-) m/z 57.00 " 100.00% 57

85 5000- ------- — n i ■ ■

30.20 30.40 30.60 30.80 31.00 —r50 1TT i r ■ 3.141 183............................................. m/z ' r । ■ TIT । > । । > । i । T > । T । > T । TIT । । । । । । T 43.05 77.00% miz-? 100___150___ 200. 250 300 350 400 450 Abundance #4’2196: Heptadecane, 2,6,10,15-tetramethyl- i 57

5000 85 1PPer--=----140 30.20 30.40 30.60 30.80 31.00

443 m/z 71.00 70.32% ,| j1141 183 211 268 296 ■ ' i FIPTTTTITIT TTI. 7 miz-> 50 100 150 200 250 300 350 400 450 Abundance #42201; Heneicosane 57 30.20 30.40 30.60 30.80 31.00 85 5000 m/z 85.05 51.09%

113 ■ ■ i ■ ■ ■ • i ■ 141, _ 268 296 .......................... miz-? 50 100 150 200 250 300 350 400 450 Abundance #74491: Dotriacontane 57 30.20 30.40 30.60 30.80 Stop m/z 41.05 36.20% 5000 85

I II113 i 141 , 196 281 422 450 444 APPpAPAA I TI———m/TTTTTTTTTTTTTT r-i—r—j—i—r-i—i—|—r m/z—> 50 100 150 200 250 300 350 400 450 30.20 30.40 30.60 30.80 31.00

28664.D GCMS1126.M Fri Dec 07 15:53:54 2001 Page 4

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