NYC-WTC_000035135
Laboratory report noting di-n-butylphthalate detection and low pH with recovery data for sample AD28694.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis comments for sample AD28691, Dec 2001
Machine-extracted title · confidence 100%Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28691.
NYC-WTC_000035052–000035071Folder label: “GCMS X 11/24/01 A 12/4/01”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0401\28691.D Vial: 11 Acq On 4 Dec 2001 10:08 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Acetic acid, octadecyl ester Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 31.80 0.47 ug/1 107718 Chrysene-dl2 33.04 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 2 1-Nonadecanol 284 C19H40O 001454-84-8 76 3 1-Nonadecene 266 C19H38 018435-45-5 64 4 1-Eicosanol 298 C20H42O 000629-96-9 62 Abundance Scan 2914 (31.796 min): 28691..D (-) m/z 43.05 100.00% 43 83 57 97 69 5000 111 —|T TTTm TTT TI—T .1 । , r .1 125 , | TTT ill TIUi 111I —l—1139153. .. 207—.... 31.40 31.60 31.80 32.00 32.20 m/z 83.00 70.23% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #73048: Acetic acid, octadecyl ester 43
5000 61 83 97 —A. — 31,40 31.60 31.80 32.00 32.20 m/z 111 57.00 60.40%
' ' i ' ' 1 125 139 224 252 I ' ' ' ' i ' ' ' ' i ■ ' ' b i ■ ■ ■ ■ i ' 1 ' ■ i ' ' ' 1 I ' ' 1 ' i ' '
1 mlz—> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #40236:1-Nonadecanol 55 83 69 97 117 1‘ I"1. '. 1. TT '~r 31.40 31.60 31.80 32.00 32.20 5000 m/z55.00 60.14% 111 31 42 125 ........ ........... ..... 238.... , 1 ' t 1 । ‘I‘ 11 U m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #37066:1-Nonadecene TPP I 1 1 ■ ■ i ' ■ • ' i ' ' 55 83 97 31.40 31.60 31.80 32.00 32.20 69 59.97% m/z 60.95 111 5000
125 | 238 266 — ■ ■ i ■ ‘ I ■ 11 T 1 TIE ' I ' ' ' ■ i ' 1 ' ' I ' ' ' 1 i ' ' ' ' P ' ■ • i ' ' 1 b i ■ ■ ■ ■ i ' ' ' TET 1 1 1. ' 1 I ' ' m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 31.40 31.60 31.80 32.00 32.20
28691.D GCMS1126.M Thu Dec 06 13:26:46 2001 Page 8
NYC-WTC_000035065
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