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GCMS results log, sample AD26985, Dec 11 2001

Machine-extracted title · confidence 95%

Laboratory report for GCMS analysis of sample AD26985 completed on December 11, 2001, showing surrogate recovery.

NYC-WTC_000032400–000032426

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032417
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Cyclopentanecarboxylic acid, 2 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.59 2.06 ng/uL 743670 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11N02 040482-05-1 43 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 43 3 1-Hexene/ 2-methyl- 98 C7H14 006094-02-6 38 4 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 38 Abundance Scan 2699 (29.588 min): 26986 D (-) m/ z 56.10 100.00% 55

5000 41 73 J I

I ■ ■ i ■ ■ ■ ' P ' r1AZ 101115128143157171185 213 tT 312 I • ' ' ' I IT 29.20 29.40 29.60 29.80 30.00 m/ z 57.10 46.69% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5212: Cyciopentanecarboxylic acid, 2-amino-, trans- 56 i

5000- ‘I M' I' ' ' ' 29.20 29.40 29.60 29.80 30.00 m/ z 43.10 37.97% 30 100 129

m/z-> .1 . I ■ i' ■ • ■ । ■ 1' । ■ 20 I 7084 TTm I • '' ’ I I'''' I T’ IIT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 I ■ ' • ' I' rr. j

Abundance

5000- 56 #521S; Cyciopentanecarboxylic acid. 2-amino-. cis-

"I M Tur 29.20 29.40 29.60 29.80 30.00 m/ z 41.10 36.09%

30 129 I . 70 84 100 i I ' i ■ ■' ■ i' ■'' i ■ ■ ‘ ।■ ' i'1 . I P I I I | I < I I | I I . I ] . I I I | . > > I | l•■•'I•' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261: 1-Hexene, 2-methyl- ‘i 56 29.20 29.4C 29.60 29.80 30.00 m/ Z 55.10 29.06% 41 5000 27 70 98 1 ■ ■ । ■ ■ ■ ■ । • ■ l m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

26986.D NP112701.M Tue Dec 11 14:51:35 2001 Page 9

NYC-WTC_000032417

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NYC-WTC_000032417Source: NYC Law Department, mirrored locally

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