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GCMS results log, sample AD26991, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26991 completed on December 11, 2001.

NYC-WTC_000032462–000032480

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

■ Data File C:\HPCHEM\l\DATA\DEC0601\26991.D Vial: 17 Acq On 7 Dec 2001 12:43 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ***************************************************** * ** * ** * ** * * *** * * Peak Number 3 Cyclopentanecarboxylic acid, 2 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.59 0.91 ng/uL 262827 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 43 2 Cyclopentanecarboxylic acid, 2-amin 12 9 C6H11NO2 037910-65-9 43 3 Oxirane, 2, 3-bis(1-methylethyl)-, t 128 C8H160 054644-32-5 37 4 1-Hexene, 2 -methyl- 98 C7H14 006094-02-6 35 Abundance Scan 2699 (29.589 min): 26991 .D (-) m/ z 56.10 100.00% 56

5000- 43 73 257 ‘d

m/z-> i" ’1P1 20 40 60 +7 1011 1122 । . 157171 185, , . 213 2~l 9 80 100 120 140 160 180 200 220 240 260 280 300 312 TIT s 29.20 29.40 29.60 29.80 30.00 m/ Z 57.10 52.78% Abundance #5212: Cyclopentanecarboxylic acid, 2-amino-, trans­ 55

5000 29.20 29.40 29.60 29.80 30.00 m/z 43.10 42.35% 30 69 82 100 129 i • ■ ■ • i •• 1 | _____ I ,0EIT"TEETEEEITETTTT T‘‘ 1..<.I... . P > . . I .... 1 .... 1 .... I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5218: Cyclopentanecarboxylic acid, 2-amino-. cis­ 56 A 29.20 29.40 29.60 29.80 30.00 5000 m/z 41.10 37.60%

30 ' 69 82 100 129

.... Us _ i TTP T I ■ 1‘ --T‘EEIIEII‘TEE-ITETEII"EEIT"EEIIIEEIItIET P I I 11 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans-

41 56 29.20 29.40 29.60 29.80 30.00 m/z 55.10 29.92% 5000

i miz-> — 113 128......... 73

r- ■ 111 ’ • > < I« • < < I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 l ■ ' ■ • I ''11 I . LA TIT 29.20 29.40 29.60 29.80 30.00

26991.D NP112701.M Tue Dec 11 14:54:24 2001. Page 3

NYC-WTC_000032472

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