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GCMS results log, sample AD26991, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD26991 completed on December 11, 2001.

NYC-WTC_000032462–000032480

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 601\26991.D Vial: 17 Acq On 7 Dec 2001 12:43 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Eicosane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

30.77 0.42 ng/uL 120174 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 2 Heptadecane 240 C17H36 000629-78-7 3 Hexadecane 226 C16H34 000544-76-3 72 4 Pentadecane 212 C15H32 _______ 000629-62-9 64 Abundance Scan 2828 (30.772 min): 26991.D (-) m/z 57.10 100.00% 57

43 71 5000 85 / ‘i II IT 30.40 30.60 30.80 31.00 31.20 : - ? 113 m/z 43.1.0 67.04% m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72323: Eicosane 43 57

5000 71 r II 85 30.40 30.60 30.80 31.00 31.20 m/z 71.05 55.90% । • • i • ' lar__ 11 i ■ ' Tui 22 113 127 141 .................................... . m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71191: Heptadecane 43 57 111 \ IT 71 30.40 30.60 30.80 31.00 31.20 5000 m/z 85.05 38.69% 85

99 113 127 141 240 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 —........................... Abundance #70789: Hexadecane 43 57 30.40 30.60 30.80 31.00 31.20 m/z 41.10 31.23% 71 5000 - 85

.40— - 1— 99113 127 226 m/z-> 60 80 100 120 140 160 180 200 220 240 260 280 30.40 30.60 30.80 31.00 31.20

26991 .D NP112701.M Tue Dec 11 14:54:26 2001 Page 4

NYC-WTC_000032473

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NYC-WTC_000032473Source: NYC Law Department, mirrored locally

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