GCMS results log, sample AD26991, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 6 01\2 6 9 91.D Vial: 17 Acq On 7 Dec 2001 12:43 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 1-Hexene, 5-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.72 0.59 ng/uL 170499 Chrysene-dl2 33.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexene, 5-methyl- 98 C7H14 003524-73-0 27 2 Piperidin-4-carboxylic acid 129 C6H11NO2 000498-94-2 23 3 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 17 4 2-Decene, 9-methyl-, (Z) - 154 C11H22 074630-24-3 17 Abundance 7 Scan 2931 (31.717 min): 26991 .D (-) m/z 5 6.10 100.00% 56

5000 43 73 TE‘/ E"T

m/z-> 20 I • • , l P”' 40 LLul6527 60 80 100 117 । — 129

120 140 160 180 200 185.................. 267 25 220 240 260 280 31.40 31.60 31.80 32.00 m/z 57.10 49.52% Abundance #63239: 1-Hexene, 5-methyl- 56 41

5000 PTm 31.40 31.60 31.80 32.00 27 70 m/z 43.10 44.65% i LI । ■ ■ ■ ■ । ■ ■ 83,98 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #5228: Piperidin-4-carboxylic add 56

31.40 31.60 31.80 32.00 5000 m/ z 41.10 38.28% 30 42 84 129 100 im/z-> — 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #28775: Pentadecane, 8-methylene- i AA ■ ' ■ ■ i

56 31.40 31.60 31.80 32.00 m/z 55.10 29.10% 5000- 69 84

m/z-> 27 । .i . । । r. 20 40 .27112125.140 60 80 100 120 140 196 224 ■ ■ i ■ ■ ■ • । > • • ■ । ■ ■ • ■ । * ■ ■ ■ । • ■ • ■ । • • ■ ■ । 160 180 200 220 240 260 280 < ■ ' i ■ ' ' i ' X—. , 31.40 31.60 31.80 32.00

26991.D NP112701.M Tue Dec 11 14:54:28 2001 Page 5

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